Carbon addition effects on microstructure and small-scale hardness for Ti(C,N)-FeNi cermets

The current study investigates the influence of carbon addition on the microstructural and micromechanical properties of Ti(C,N)-FeNi cermets with different ceramic/metal phase ratios. Evaluation of small-scale hardness is conducted by using high speed nanoindentation in conjunction with statistical...

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Bibliographic Details
Authors: Besharatloo, H.; Nicolás Morillas, Maria de; Wheeler, J.M.; Mateo García, Antonio Manuel|||0000-0001-8336-6128; Ferrari, Begoña; Gordo Odériz, Elena; Llanes Pitarch, Luis Miguel|||0000-0003-1054-1073; Roa Rovira, Joan Josep|||0000-0002-7440-0766
Format: Article
Publication date:2019
Country:España
Institution:Universitat Politècnica de Catalunya (UPC)
Repository:UPCommons. Portal del coneixement obert de la UPC
Language:English
OAI Identifier:oai:upcommons.upc.edu:2117/177340
Online Access:https://hdl.handle.net/2117/177340
https://dx.doi.org/10.1016/j.ijrmhm.2019.105064
Access Level:Open access
Keyword:Materials -- Mechanical properties
Cermet
High speed indentation
Hardness
Mechanical mapping
Massive indentation
Statistical analysis
Materials -- Propietats mecàniques
Àrees temàtiques de la UPC::Enginyeria dels materials
Description
Summary:The current study investigates the influence of carbon addition on the microstructural and micromechanical properties of Ti(C,N)-FeNi cermets with different ceramic/metal phase ratios. Evaluation of small-scale hardness is conducted by using high speed nanoindentation in conjunction with statistical analysis. It allows to gather extremely large data sets (40,000 imprints per grade and condition); and thus, detailed hardness mapping at the microstructure length scale. Subsequent statistical analysis was done by considering three mechanically distinct phases: Ti(C,N) particles, the metallic binder, and one exhibiting the composite behaviour (i.e.imprints probing two-phase regions). In general, it is found that porosity amount is reduced as ceramic/metal phase ratio decreases and carbon is added. Carbon addition is also observed to rise small-scale hardness, but only for two of the defined phases: metallic binder and the composite one. Similar trends are observed regarding the influence of ceramic/metal phase ratio and carbon addition on the inverse hardness-fracture toughness correlation measured under high applied loads.